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BULLETIN OF THE CHINESE CERAMIC SOCIETY ›› 2020, Vol. 39 ›› Issue (12): 3881-3888.

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Preparation of Rice Husk Ash and Its Effect on Mechanical Properties of Geopolymer

LIU Zhenzheng1,2,3, XIE Chunlei1,2,3, WANG Xueying1,2,3, GUO Liang4, WU Yueyue4, CHEN Qin5, DUAN Ping4   

  1. 1. Inner Mongolia Communication Engineering Quality Supervision Bureau, Hohhot 010051, China;
    2. Key Laboratory of Transport Industry of Management, Control and Cycle Repair Technology for Traffic Network Facilitates in Ecological Security Barrier Area, Hohhot 010051, China;
    3. Inner Mongolia Key Laboratory of Road Structure and Materials, Hohhot 010051, China;
    4. Faculty of Materials Science and Chemistry, China University of Geosciences (Wuhan), Wuhan 430074, China;
    5. Wuhan Hanyang Municipal Construction Group Company Limited, Wuhan 430050, China
  • Published:2021-02-01

Abstract: Using rice husk (RH) as raw material, the differences of properties and structures of rice husk ash (RHA) prepared under different treatment conditions and the effects on the mechanical properties of metakaolin-based geopolymer were studied. The optimum preparation conditions of RHA were determined. The results show that hydrochloric acid pretreatment significantly improves the purity of amorphous SiO2 in RHA as high as 98.354% (mass fraction). The RH pretreated by acid is calcined completely by calcining 60 min at 550 ℃ and the reaction activity of RHA is the highest. RHA treated by acid makes the pore structure of geopolymers denser and the 28 d compressive strength of 550 ℃ RHA geopolymer (10% (mass fraction) RHA+90% (mass fraction) metakaolin) is the highest, which is 53.3 MPa. Through comprehensive impact analysis, the optimum preparation conditions of RHA are as follows: immersed in 2.5% (mass fraction) hydrochloric acid for 1 h and calcined at 550 ℃ for 1 h.

Key words: rice husk ash, acid treatment, calcination temperature, geopolymer, mechanical property

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