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BULLETIN OF THE CHINESE CERAMIC SOCIETY ›› 2008, Vol. 27 ›› Issue (1): 16-19.

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Preparation and Characterization of Phase Change Materials by Solid-State Chemical Reaction at Low Heating Temperature

CHAI Hui;ZENG Ling-ke;WANG Hui;LIU Ping-an;CHENG Xiao-su;SHUI An-ze   

  • Online:2008-02-15 Published:2021-01-15

Abstract: The synthesis of SiO2 coated palmitic acid (PA) nanoparticles via one-step,low heating temperature solid-state chemical reaction is reported. Analytical results of Infrared spectroscopy and X-ray diffraction prove that the palmitic acid (PA) was coated with a layer of SiO2.Morphology of scanning electron microscopy suggests that the sample is comprised of sphere-like nanoparticals with average diameter about 200nm.The as-prepared sample has been studied with differential scanning calorimetry (DSC).The transformation temperatures is 51.9℃and the fusion enthalpy are 3.36×104J/mol.The result shows that the sample possesses reasonable thermal property as a phase change material for latent heat energy storage application.

Key words: solid-state reaction%fatty acid%phase transition materials%composite

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