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硅酸盐通报 ›› 2017, Vol. 36 ›› Issue (11): 3759-3765.

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SnO2纳米花的水热合成及其光催化性能研究

胡文全;袁晓光;王岩;冯毅毅   

  1. 沈阳工业大学材料科学与工程学院,沈阳 110870;辽宁工程技术大学材料科学与工程学院,阜新 123000;沈阳工业大学材料科学与工程学院,沈阳,110870;辽宁工程技术大学材料科学与工程学院,阜新,123000
  • 出版日期:2017-11-15 发布日期:2021-01-18

Hydrothermal Synthesis and Photocatalytic Properties of SnO2 Nanoflowers

HU Wen-quan;YUAN Xiao-guang;WANG Yan;FENG Yi-yi   

  • Online:2017-11-15 Published:2021-01-18

摘要: 采用简单水热法合成出了成分纯净、形貌良好、光催化性能优良的SnO2纳米花,并对合成产物进行物相分析、形貌观察、微观结构分析、比表面积测试及光催化性能测试.结果表明:该SnO2纳米材料形貌均一,呈花形,花片厚度为5 nm左右.合成产物为四方金红石相结构,成分纯净、结晶性好,比表面积大,对亚甲基蓝、甲基橙、罗丹明B、刚果红四种有机染料具有良好的光催化活性,降解时间短,降解率高.该合成产物作为光催化剂具有可重用性.

关键词: 水热法;SnO2;纳米花;光催化性能

Abstract: Large amounts of SnO2 nanoflowers with pure composition,good morphology and excellent photocatalytic performance were successfully obtained through a simple and effective hydrothermal method. The phase analysis, morphology, microstructure, specific surface area and photocatalytic properties were characterized. The results show that the morphology of SnO2 nanoflowers are uniform and the thickness of single nanopetal is about 5 nm. The synthesized products are tetragonal rutile structure with high purity,well crystallinity and high specific surface area. The SnO2 nanoflowers possess excellent photocatalytic activity for methylene blue,methyl orange,rhodamine B,congo red. The degradation time is short and the degradation rate is high. As a photocatalyst,the prepared SnO2 nanoflowers have reusability.

Key words: hydrothermal method;SnO2;nanoflower;photocatalytic property

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