欢迎访问《硅酸盐通报》官方网站,今天是

硅酸盐通报 ›› 2010, Vol. 29 ›› Issue (1): 209-213.

• • 上一篇    下一篇

化学法制备ZA复合粉体的研究

田晓利;薛群虎;薛崇勃   

  1. 西安建筑科技大学材料科学与工程学院,西安,710055;河南濮阳濮耐高温材料(集团)股份有限公司,濮阳,457100;西安建筑科技大学材料科学与工程学院,西安,710055;河南濮阳濮耐高温材料(集团)股份有限公司,濮阳,457100
  • 出版日期:2010-02-15 发布日期:2021-01-18
  • 基金资助:
    陕西省国家重点学科培育学科资助

Study on Alumina-zirconia Composite Powder Prepared by Chemical Methods

TIAN Xiao-li;XUE Qun-hu;XUE Chong-bo   

  • Online:2010-02-15 Published:2021-01-18

摘要: 采用溶胶-凝胶法和共沉淀法两种化学方法制备了氧化铝-氧化锆复合粉体,并对其进行表征:采用激光粒度分析仪测定粉体粒径及粒度分布,X射线衍射仪(XRD)进行矿物相组成分析,扫描电子显微镜(SEM)观察微观下氧化铝与氧化锆的分布情况.结果表明:溶胶-凝胶法制备的粉体相对于共沉淀法制备的粉体粒度较细,四方相氧化锆含量高,而且氧化铝和氧化锆分散较均匀.

关键词: 溶胶-凝胶法;共沉淀法;氧化铝-氧化锆复合粉体

Abstract: Alumina-zirconia composite powders were prepared by two chemical methods, which were Sol-gel method and co-precipitation method, and then characterized by some equipments: size of the granularity was expressed by laser particle size analyzer, phase composition was analyzed by X-ray diffraction (XRD) and distribution of alumina and zirconia at microscopic view was observed by scanning electron microscope (SEM). The experimental results show that compared with co-precipitation method, the powder from Sol-gel method was preferable, of which the granularity was much thinner, the content of tetragonal zirconia was much higher and the distribution of alumina and zirconia was much evener.

Key words: Sol-gel method;co-precipitation method;alumina-zirconia composite powder

中图分类号: