微波水热法合成Mn掺杂BaTiO_3纳米粉体

硅酸盐通报 ›› 2010, Vol. 29 ›› Issue (1): 107-111.

微波水热法合成Mn掺杂BaTiO_3纳米粉体

马麦霞;张光霞

廊坊师范学院化学与材料科学学院,廊坊,065000

出版日期:2010-02-15 发布日期:2021-01-18
基金资助:
廊坊师范学院青年基金(LSZQ200802)

Preparation of Mn-doped Barium Titanate Nano-powder by Microwave-hydrothermal Method

MA Mai-xia;ZHANG Guang-xia

Online:2010-02-15 Published:2021-01-18

摘要/Abstract

摘要： 以Ti(OC_4H_9)_4 、Ba(NO_3)_2 和C_4H_6MnO_4·4H_2O为原料,采用微波水热法合成了Mn掺杂的BaTiO_3纳米粉体.通过X射线衍射(XRD)和扫描电子显微镜(SEM)对产物进行了表征.并研究了影响Mn掺杂BaTiO_3晶体生长和形貌的主要影响因素.实验结果表明:掺杂量为1.0%,反应时间为30 min,烘箱干燥温度为82 ℃,能制备出单一的粒径均匀的掺Mn的BaTiO_3纳米粉体,且粉体的粒径尺寸约为100 nm.

关键词: Mn掺杂的BaTiO_3;纳米粉体;微波水热法

Abstract: The Mn-doped barium titanate nano-powders were synthesized by Microwave-hydrothermal Method, in which Ti(OC_4H_9)_4 、Ba(NO_3)_2 and C_4H_6MnO_4·4H_2O compounds were used as raw materials. The Mn-doped Barium Titanate nano-powders were characterized by means of X-ray diffraction (XRD) and scanning electron microscope (SEM). The primary effects of processing parameters on the growth and morphology of the Mn-doped Barium Titanate were studied. The experimental results showed that the Mn-doped Barium Titanate of pure phase and uniform size was obtained when the concentration of Mn, the reaction time and drying temperature were 1.0%, 30 min and 82 ℃, respectively. And the size of the Mn-doped Barium Titanate powders was about 100 nm.

Key words: Mn-doped barium titanate;nano-powders;microwave-hydrothermal method

中图分类号:

TF12

马麦霞;张光霞. 微波水热法合成Mn掺杂BaTiO_3纳米粉体[J]. 硅酸盐通报, 2010, 29(1): 107-111.

MA Mai-xia;ZHANG Guang-xia. Preparation of Mn-doped Barium Titanate Nano-powder by Microwave-hydrothermal Method[J]. BULLETIN OF THE CHINESE CERAMIC SOCIETY, 2010, 29(1): 107-111.

[1]	韦华栋;袁静;洪永鹏;张金星;孟涛;赵羽习;沈林昌. 装修垃圾除尘粉的特性及其对水泥净浆力学性能的影响[J]. 硅酸盐通报, 2020, 39(5): 1517-1524.
[2]	王晨;董磊;尚福亮;高玲;杨海涛. Nb2O5掺杂ZnO超高致密度陶瓷靶材的制备[J]. 硅酸盐通报, 2017, 36(9): 3150-3154.
[3]	王艺慈;霍晓更;罗果萍;王永斌;张芳. Cr2O3、Fe2O3对高炉渣粘熔特性的影响[J]. 硅酸盐通报, 2017, 36(2): 701-705.
[4]	史继媛;刘宗明;李金凯;李莉;赵蔚琳. 导热油基TiO2纳米流体热物性研究[J]. 硅酸盐通报, 2016, 35(10): 3324-3329.
[5]	刘慧敏;孙晶;张敏;潘柳;张鑫洋;于文生. 柠檬酸凝胶燃烧法制备GGG∶Eu3+,Bi3+多晶发光粉体及其表征[J]. 硅酸盐通报, 2016, 35(3): 716-720.
[6]	吴昊;史春燕;付晓辉;赵婉瑜;范冰冰;张锐. 低温水热法制备纳米氧化锆粉体[J]. 硅酸盐通报, 2015, 34(11): 3247-3250.
[7]	张彦娜;朱宪忠;王杰. 共沉淀-熔盐法制备YAG荧光粉的研究[J]. 硅酸盐通报, 2015, 34(3): 684-687.
[8]	李丹;姜兴斌;顾毅;李辉;蒋鑫;马春生;高莹;周连科. 陶瓷坩埚在水雾化法制造触媒合金粉中的应用研究[J]. 硅酸盐通报, 2014, 33(11): 2992-2994.
[9]	徐明晗;鞠银燕;宋杰光;王芳. 湿法球磨制备超细钴蓝粉体的研究[J]. 硅酸盐通报, 2014, 33(10): 2716-2719.
[10]	胡继林;胡传跃;刘鑫;田修营. SiC粉末制备技术及其烧结助剂的研究进展[J]. 硅酸盐通报, 2014, 33(9): 2280-2284.
[11]	王舟;沈湘黔;李东红;胡文豪. 尿酶对共沉淀法制备球形α-氧化铝的影响[J]. 硅酸盐通报, 2014, 33(9): 2346-2349.
[12]	刘世鹏. 反相悬浮体系制备高纯多孔二氧化硅微球[J]. 硅酸盐通报, 2014, 33(9): 2370-2374.
[13]	石连水;张林;陈萍华;周雪珍;赵夫健;李永绣. 机械化学法制备ZrO2纳米粉体的工艺研究[J]. 硅酸盐通报, 2014, 33(6): 1443-1446.
[14]	林启权;龙燕萍;董文正;姜滔;彭传东. Y2O3掺杂对17Ni/(NiFe2O4-10NiO)金属陶瓷高温氧化性能的影响[J]. 硅酸盐通报, 2014, 33(4): 890-894.
[15]	王彬彬;范冰冰;陈勇强;张锐. 原位化学沉积法制备镍包覆碳化硅颗粒复合粉体[J]. 硅酸盐通报, 2014, 33(3): 629-634.