负温环境下快硬早强胶凝材料的早期性能研究进展

doi:10.16552/j.cnki.issn1001-1625.2025.0357

摘要/Abstract

摘要： 抢修抢建工程要求胶凝材料必须具备快硬早强特性,在高海拔、高纬度地区及冬季严寒天气下,胶凝材料需适应负温环境。传统胶凝材料在此环境下无法正常水化,导致不凝固且无强度。磷酸镁水泥、硫铝酸盐水泥、碱激发矿渣胶凝材料、复合胶凝材料具有快凝快硬、水化放热集中、早强高强的特性,展现出应用于负温环境的潜力。本文综述了负温环境下快硬早强胶凝材料早期性能的研究进展,着重分析了负温环境下原材料的种类及性质、原材料之间的配比对磷酸镁水泥早期强度形成的影响,以及胶凝材料组分、防冻剂、早强剂及纳米材料等对硫铝酸盐水泥早期性能的改善效果。此外,本文还对未来负温环境下快硬早强胶凝材料的发展进行了展望。

关键词: 胶凝材料, 负温环境, 强度, 磷酸镁水泥, 硫铝酸盐水泥

Abstract: The urgent repair and construction engineering requires that the cementitious material must have the characteristics of rapid hardening and early strength, and the cementitious material must face negative temperature environment in high altitude-high latitude areas and cold weather in winter. Traditional cementitious material cannot hydrate normally in this environment, and do not solidify and without strength. Magnesium phosphate cement, sulphoaluminate cement, alkali-activated slag cementitious material and composite cementitious material have the characteristics of fast setting and rapid hardening, hydration heat release concentration, early strength and high strength, showing the potential of application in negative temperature environment. In this paper, the research progress on the early age properties of rapid hardening and early strength cementitious materials under negative temperature environment was reviewed. The effects of the types and properties of raw materials and the ratio of raw materials on the early strength formation of magnesium phosphate cement under negative temperature environment were emphatically analyzed, as well as the improvement effects of cementing material components, antifreeze, early strength agents and nanomaterials on the early age property of sulphoaluminate cement. In addition, the future development of rapid hardening and early strength cementitious material under negative temperature environment was prospected.

Key words: cementitious material, negative temperature environment, strength, magnesium phosphate cement, sulphoaluminate cement

中图分类号:

TU528

张超, 王志航, 王超, 聂良学, 李炳辰, 罗鑫, 陈涛. 负温环境下快硬早强胶凝材料的早期性能研究进展[J]. 硅酸盐通报, 2025, 44(10): 3503-3516.

ZHANG Chao, WANG Zhihang, WANG Chao, NIE Liangxue, LI Bingchen, LUO Xin, CHEN Tao. Early Age Properties of Rapid Hardening and Early Strength Cementitious Material at Negative Temperature Environment: a Review[J]. BULLETIN OF THE CHINESE CERAMIC SOCIETY, 2025, 44(10): 3503-3516.

参考文献

[1] 陈歆, 刘文, 崔安琪, 等. 高海拔地区低温成型磷酸镁水泥砂浆力学与抗冻性能[J]. 材料导报, 2024, 38(17): 53-61.
CHEN X, LIU W, CUI A Q, et al. Mechanical properties and freeze-thaw cycling resistance of magnesium phosphate cement mortar prepared at low temperatures in highland regions[J]. Materials Reports, 2024, 38(17): 53-61 (in Chinese).
[2] 张彤, 王志航, 白二雷, 等. 玄武岩纤维增强早强混凝土的早期动态力学性能[J]. 化工新型材料, 2023, 51(增刊2): 487-492.
ZHANG T, WANG Z H, BAI E L, et al. Early dynamic mechanical properties of basalt fiber reinforced early strength concrete[J]. New Chemical Materials, 2023, 51(supplement 2): 487-492 (in Chinese).
[3] WANG Z J, LI W J, ZHAO M L. Effect of antifreeze on the low-temperature properties of magnesium phosphate cement concrete[J]. Key Engineering Materials, 2024, 998: 103-110.
[4] 韦宇, 周新涛, 黄静, 等. 缓凝剂对磷酸镁水泥性能及其水化机制影响研究进展[J]. 材料导报, 2022, 36(4): 77-83.
WEI Y, ZHOU X T, HUANG J, et al. Research progress on the effects of retarders on the properties and hydration mechanism of magnesium phosphate cement[J]. Materials Reports, 2022, 36(4): 77-83 (in Chinese).
[5] WANG Z H, BAI E L, LIU C J, et al. Early age dynamic mechanical properties of basalt fiber reinforced early strength concrete[J]. Structural Concrete, 2023, 24(6): 7648-7659.
[6] 吕炎, 白二雷, 王志航, 等. 粉煤灰-矿渣基地聚物混凝土不同龄期动态力学性能[J]. 空军工程大学学报, 2022, 23(6): 99-106.
LYU Y, BAI E L, WANG Z H, et al. Dynamic mechanical properties of fly ash-slag based polymer concrete at different ages [J]. Journal of Air Force Engineering University, 2022, 23(6): 99-106 (in Chinese).
[7] 吕炎, 白二雷, 王志航, 等. 低温养护对环氧树脂基砂浆早期性能的影响及机理[J]. 材料导报, 2024, 38(5): 102-107.
LYU Y, BAI E L, WANG Z H, et al. Effect and mechanism of low temperature curing on the early performance of epoxy resin based mortar[J]. Materials Reports, 2024, 38(5): 102-107 (in Chinese).
[8] QIAN W Y, SUN W, GUO S, et al. Effect of temperature variation on bonding properties of magnesium potassium phosphate cement: a multiscale analysis[J]. Case Studies in Construction Materials, 2024, 21: e03993.
[9] 田婷, 张爱, 李国新, 等. 氧化钙对硅酸盐水泥-铝酸盐水泥-硫酸钙体系低温水化性能的影响[J]. 硅酸盐通报, 2015, 34(12): 3670-3675.
TIAN T, ZHANG A, LI G X, et al. Influence of calcium oxide on the hydration performance of Portland cement-aluminate cement-gypsum ternary system at low temperature[J]. Bulletin of the Chinese Ceramic Society, 2015, 34(12): 3670-3675 (in Chinese).
[10] 方仁义, 于蕾, 范波, 等. 低温暴露养护条件下混凝土强度增长规律研究[J]. 水利水电技术(中英文), 2024, 55(增刊 2): 733-739.
FANG R Y, YU L, FAN B, et al. Study on the law of concrete strength growth under low temperature exposure and curing conditions[J]. Water Resources and Hydropower Engineering, 2024, 55(supplement 2): 733-739 (in Chinese).
[11] 王霄翔, 谢剑, 李培冬, 等. 超低温冻融循环后混凝土应力-应变全曲线试验研究[J]. 水利水电技术, 2014, 45(8): 153-158.
WANG X X, XIE J, LI P D, et al. Experimental study on complete stress-strain curve of concrete after freeze-thaw cycles under extra-low temperatures[J]. Water Resources and Hydropower Engineering, 2014, 45(8): 153-158 (in Chinese).
[12] LIU K X, YU W X, JIN L, et al. Influence of moisture content on compressive properties of concrete at cryogenic temperatures: tests and formulations[J]. Journal of Building Engineering, 2025, 100: 111771.
[13] YUAN J, ZHANG Z P, CHEN X, et al. Long-term performance of magnesium phosphate cement concrete prepared in the winter[J]. European Journal of Environmental and Civil Engineering, 2025, 29(1): 176-200.
[14] 陶琦, 王岩. 负温下磷酸镁水泥混凝土的力学性能与抗冻性能[J]. 冰川冻土, 2018, 40(6): 1181-1186.
TAO Q, WANG Y. Mechanical properties and frost resistance of magnesium phosphate cement concrete under negative temperature[J]. Journal of Glaciology and Geocryology, 2018, 40(6): 1181-1186 (in Chinese).
[15] JIA X W, LI J M, WANG P, et al. Preparation and mechanical properties of magnesium phosphate cement for rapid construction repair in ice and snow[J]. Construction and Building Materials, 2019, 229: 116927.
[16] 张志超. 严寒环境冰水拌和磷酸镁水泥基材料的性能研究[D]. 哈尔滨: 哈尔滨工业大学, 2022.
ZHANG Z C. Study on properties of magnesium phosphate cement-based materials mixed with ice water in cold environment[D]. Harbin: Harbin Institute of Technology, 2022 (in Chinese).
[17] 王平. 严寒环境下磷酸镁水泥的反应进程与力学性能调控[D]. 重庆: 重庆大学, 2020.
WANG P. Reaction process and mechanical properties regulation of magnesium phosphate cement in severe cold environment[D]. Chongqing: Chongqing University, 2020 (in Chinese).
[18] LUO X Z, LAI Z Y, LIU Z, et al. Effect of modified magnesium oxide on the properties of magnesium phosphate cement under a negative temperature environment[J]. Materials, 2022, 15(24): 9047.
[19] 杜杰贵, 王雄锋, 陈波, 等. 磷酸镁水泥在快速修补工程中的应用研究进展[J]. 施工技术(中英文), 2022, 51(15): 6-11.
DU J G, WANG X F, CHEN B, et al. Review of magnesium phosphate cement applied in rapid repair engineering[J]. Construction Technology, 2022, 51(15): 6-11 (in Chinese).
[20] ZHAO Z H, CAI X H, CHEN F, et al. Effect of wollastonite content on rheology and mechanical properties of 3D printed magnesium potassium phosphate cement-based material of MgO-SiO₂-K₂HPO₄[J]. Construction and Building Materials, 2025, 458: 139729.
[21] 张子鹏. 早期冻融对负温制备磷酸镁水泥基材料后期性能的影响研究[D]. 哈尔滨: 哈尔滨工业大学, 2023.
ZHANG Z P. Effect of early freeze-thaw on late performance of magnesium phosphate cement-based materials prepared at negative temperature[D]. Harbin: Harbin Institute of Technology, 2023 (in Chinese).
[22] 杨奉源, 赖振宇, 李军, 等. 负温环境下复合磷酸盐对磷酸镁水泥性能的影响[J]. 新型建筑材料, 2024, 51(8): 123-129+135.
YANG F Y, LAI Z Y, LI J, et al. The effect of composite phosphates on the properties of magnesium phosphate cement under negative temperature environment[J]. New Building Materials, 2024, 51(8): 123-129+135 (in Chinese).
[23] 潘明杰, 郭金波, 刘润清. 负温环境下磷酸二氢钠对磷酸镁水泥力学性能的影响[J]. 辽宁化工, 2024, 53(8): 1199-1202.
PAN M J, GUO J B, LIU R Q. Effect of sodium dihydrogen phosphate on mechanical properties of magnesium phosphate cement under negative temperature environment[J]. Liaoning Chemical Industry, 2024, 53(8): 1199-1202 (in Chinese).
[24] 李俊萌. 严寒环境抢修抢建用磷酸镁水泥混凝土的制备与力学性能研究[D]. 重庆: 重庆大学, 2020.
LI J M. Study on preparation and mechanical properties of magnesium phosphate cement concrete for emergency repair and construction in cold environment[D]. Chongqing: Chongqing University, 2020 (in Chinese).
[25] 戴民, 裴荔樵. 双组份负温磷酸镁水泥道路快速修补砂浆的制备与性能研究[J]. 新型建筑材料, 2018, 45(9): 21-24.
DAI M, PEI L Q. Study on the preparation and performance of double component negative temperature MPC road quick repair mortar[J]. New Building Materials, 2018, 45(9): 21-24 (in Chinese).
[26] 裴荔樵. 负温条件下双组份MPC快速修补材料的制备研究[D]. 沈阳: 沈阳建筑大学, 2018.
PEI L Q. Study on preparation of Two-component MPC rapid repair material under negative temperature conditions[D]. Shenyang: Shenyang Jianzhu University, 2018 (in Chinese).
[27] 汪宏涛. 高性能磷酸镁水泥基材料研究[D]. 重庆: 重庆大学, 2006.
WANG H T. Research on high performance magnesium phosphate cement-based materials[D]. Chongqing: Chongqing University, 2006 (in Chinese).
[28] 王攀龙, 高江涛. 防冻外加剂对磷酸盐水泥负温力学性能的影响[J]. 中国建材科技, 2021, 30(6): 40-42.
WANG P L, GAO J T. Effect of antifreeze admixture on mechanical properties of MPC at negative temperature[J]. China Building Materials Science & Technology, 2021, 30(6): 40-42 (in Chinese).
[29] 袁梦甜. 养护温度对粉煤灰磷酸镁修补砂浆性能影响机制研究[D]. 郑州: 中原工学院, 2023.
YUAN M T. Study on mechanism of influence of curing temperature on properties of fly ash magnesium phosphate repair mortar [D]. Zhengzhou: Zhongyuan University of Technology, 2023 (in Chinese).
[30] 王乐凡, 张继超, 郭鹏硕, 等. 严寒环境下磷酸镁水泥材料早期性能研究[J]. 空军工程大学学报, 2024, 25(5): 10-18+1.
WANG L F, ZHANG J C, GUO P S, et al. Research on early performance optimization for magnesium phosphate cement materials in severe cold environment[J]. Journal of Air Force Engineering University, 2024, 25(5): 10-18+1 (in Chinese).
[31] 谢剑, 金凌翼, 李伟, 等. 负温养护条件下钢纤维增强磷酸镁水泥复合材料力学性能[J/OL]. 复合材料学报, 2024: 1-12 (2024-12-31) [2025-03-05]. https://kns.cnki.net/KCMS/detail/detail.aspx?filename=FUHE20241230002&dbname=CJFD&dbcode=CJFQ.
XIE J, JIN L Y, LI W, et al. Mechanical properties of steel fiber reinforced magnesium phosphate cement composites under negative temperature curing conditions[J/OL]. Acta Materiae Compositae Sinica, 2024: 1-12 (2024-12-31) [2025-03-05]. https://kns.cnki.net/KCMS/detail/detail.aspx?filename=FUHE20241230002&dbname=CJFD&dbcode=CJFQ (in Chinese).
[32] 张歌. 硫铝酸盐水泥改性磷酸镁水泥的作用效果及其机理研究[D]. 西安: 西安建筑科技大学, 2016.
ZHANG G. Study on the effect and mechanism of magnesium phosphate cement modified by sulphoaluminate cement[D]. Xi’an: Xi’an University of Architecture and Technology, 2016 (in Chinese).
[33] HUANG X M, LIU G D, ZHENG Y, et al. The performance of magnesium phosphate cement in negative temperature environment: a state-of-the-art review[J]. Journal of Building Engineering, 2023, 76: 107278.
[34] LIU S J, YANG K, YU L, et al. Integrated assessment of magnesium phosphate cement repaired concrete from the perspective of mechanical, geometric and electrochemical compatibility[J]. Cement and Concrete Composites, 2025, 157: 105958.
[35] 刘文. 低温低气压环境下磷酸镁水泥基材料孔结构与抗冻性研究[D]. 哈尔滨: 哈尔滨工业大学, 2022.
LIU W. Study on pore structure and frost resistance of magnesium phosphate cement-based materials under low temperature and low air pressure[D]. Harbin: Harbin Institute of Technology, 2022 (in Chinese).
[36] 葛乾. 严寒地区自然环境下磷酸镁水泥水化与孔结构研究[D]. 哈尔滨: 哈尔滨工业大学, 2021.
GE Q. Study on hydration and pore structure of magnesium phosphate cement under natural environment in cold region[D]. Harbin: Harbin Institute of Technology, 2021 (in Chinese).
[37] JIA X W, LUO J Y, ZHANG W X, et al. Reaction characteristics and compressive strength of magnesia-phosphate cement at negative temperatures[J]. Construction and Building Materials, 2021, 305: 124819.
[38] 江丽君. 快速修补材料施工工艺与施工方法研究[D]. 沈阳: 沈阳建筑大学, 2016.
JIANG L J. Research on construction technology and construction method of rapid repair materials[D]. Shenyang: Shenyang Jianzhu University, 2016 (in Chinese).
[39] LUO S, ZHANG G F, WANG X H, et al. Investigation on the effects of EVA on the early hydration of calcium sulfoaluminate cement[J]. Construction and Building Materials, 2025, 466: 140348.
[40] LU L L, LIU Y W, LUO Q, et al. Investigation into the effect of sulfoaluminate cement on compressive strength and impermeability of Portland cement with alkali-free accelerator at low temperatures[J]. Journal of Building Engineering, 2025, 101: 111948.
[41] HUANG G P, PUDASAINEE D, GUPTA R, et al. Hydration reaction and strength development of calcium sulfoaluminate cement-based mortar cured at cold temperatures[J]. Construction and Building Materials, 2019, 224: 493-503.
[42] ZHANG G, JIANG S, LEI Y J. Optimizing anti-freezing agent on the properties of Portland cement-calcium sulphoaluminate cement system based on Taguchi-GRA method[J]. Case Studies in Construction Materials, 2024, 20: e02998.
[43] 王敬宇. 负温条件下硫铝酸盐水泥水化及性能的研究[D]. 北京: 中国建筑材料科学研究总院, 2020.
WANG J Y. Study on slurry formation and properties of sulphoaluminate under negative temperature[D]. Beijing: China Building Materials Research Institute, 2020 (in Chinese).
[44] 张鸿飞. 全负温条件下硫铝酸盐水泥性能调控及其机理研究[D]. 北京: 中国建筑材料科学研究总院, 2023.
ZHANG H F. Study on performance regulation and mechanism of sulphoaluminate cement under full negative temperature[D]. Beijing: China Building Materials Research Institute, 2023 (in Chinese).
[45] 孙华阳. 负温路面快速修补用硫铝酸盐水泥ECC性能研究[D]. 哈尔滨: 哈尔滨工业大学, 2022.
SUN H Y. Study on ECC performance of sulfoaluminate cement for rapid repair of negative temperature pavement[D]. Harbin: Harbin Institute of Technology, 2022 (in Chinese).
[46] 邓君安, 李德栋, 李启棣, 等. 硫铝酸盐早强水泥负温下的水化硬化[J]. 硅酸盐学报, 1983, 11(1): 85-94.
DENG J A, LI D D, LI Q D, et al. The hydration and hardening of high early strength sulfoaluminate cement under subzero performance[J]. Journal of the Chinese Ceramic Society, 1983, 11(1): 85-94 (in Chinese).
[47] HUO Y L, LU D, HAN X Y, et al. The role of admixed CaO in a sulphoaluminate cement system under winter environments[J]. Journal of Building Engineering, 2023, 78: 107638.
[48] 张晨. 外加剂对硫铝酸盐水泥负温性能影响及作用机理研究[D]. 哈尔滨: 哈尔滨工业大学, 2022.
ZHANG C. Effect of admixtures on negative temperature properties of sulphoaluminate cement and its mechanism[D]. Harbin: Harbin Institute of Technology, 2022 (in Chinese).
[49] 张鸿飞, 任俊儒, 叶家元, 等. 负温条件下不同溶液拌合硫铝酸盐水泥性能演化规律及机制[J]. 硅酸盐学报, 2024, 52(2): 624-640.
ZHANG H F, REN J R, YE J Y, et al. Performance evolution laws and mechanisms of calcium sulphoaluminate cement mixed with different solutions at sub-zero temperature[J]. Journal of the Chinese Ceramic Society, 2024, 52(2): 624-640 (in Chinese).
[50] 张鸿飞, 叶家元, 任俊儒, 等. -10 ℃条件下氯化钙溶液对硫铝酸盐水泥性能的影响[J]. 硅酸盐学报, 2022, 50(11): 2834-2843.
ZHANG H F, YE J Y, REN J R, et al. Effect of calcium chloride solution on performance of calcium sulphoaluminate cement at -10 ℃[J]. Journal of the Chinese Ceramic Society, 2022, 50(11): 2834-2843 (in Chinese).
[51] 李华明. 防冻剂作用下硫铝酸盐水泥负温性能及其水化热力学模拟[D]. 哈尔滨: 哈尔滨工业大学, 2020.
LI H M. Negative temperature performance and thermodynamic simulation of hydration of sulphoaluminate cement under the action of antifreeze[D]. Harbin: Harbin Institute of Technology, 2020 (in Chinese).
[52] 刘涛, 董三宝, 王丹, 等. 负温固井用锂盐-硫铝酸盐水泥浆体系[J]. 钻井液与完井液, 2024, 41(4): 496-505.
LIU T, DONG S B, WANG D, et al. Lithium salt-sulfoaluminate mud system for negative temperature cementing[J]. Drilling Fluids and Completion Fluids, 2024, 41(4): 496-505 (in Chinese).
[53] CHEN H L, LI Z H, YING G B. Improvement of the negative-temperature properties of calcium sulphoaluminate cement by three multifunctional chemical admixtures[J]. Developments in the Built Environment, 2024, 20: 100537.
[54] HUO Y L, HU S L, LU D, et al. Understanding the roles of Li₂CO₃ in a sulphoaluminate cement system at negative temperatures[J]. Case Studies in Construction Materials, 2023, 19: e02574.
[55] WANG Z H, BAI E L, XU J Y, et al. Effect of nano-SiO₂ and nano-CaCO₃ on the static and dynamic properties of concrete[J]. Scientific Reports, 2022, 12(1): 907.
[56] 李恒, 王正君, 杜英欣. 纳米SiO₂对硫铝酸盐混凝土负温力学性能与微观结构的影响[J]. 复合材料学报, 2025, 42(3): 1555-1565.
LI H, WANG Z J, DU Y X. Effect of nano-SiO₂ on negative temperature mechanical properties and microstructure of sulfoaluminate concrete[J]. Acta Materiae Compositae Sinica, 2025, 42(3): 1555-1565 (in Chinese).
[57] CHEN T, WANG Z H, BAI E L, et al. Effect of nano admixtures on the engineering properties and microstructure of sulphoaluminate cement mortar at -10 ℃[J]. Construction and Building Materials, 2023, 402: 133015.
[58] ZOU D H, WANG K, LI H Y, et al. Effect of LiAl-layered double hydroxides on hydration of calcium sulfoaluminate cement at low temperature[J]. Construction and Building Materials, 2019, 223: 910-917.
[59] 王可. 纳米锂铝类水滑石对硫铝酸盐水泥水化硬化影响研究[D]. 焦作: 河南理工大学, 2020.
WANG K. Effect of nano-lithium aluminum hydrotalcite on hydration hardening of sulphoaluminate cement[D]. Jiaozuo: Henan Polytechnic University, 2020 (in Chinese).
[60] 王敬宇, 叶家元, 程华, 等. 负10 ℃条件下缓凝剂对快硬硫铝酸盐水泥水化及强度的影响[J]. 硅酸盐学报, 2020, 48(8): 1285-1294.
WANG J Y, YE J Y, CHENG H, et al. Effect of retarder on hydration and strength of rapid-hardening calcium sulphoaluminate cement at -10 ℃[J]. Journal of the Chinese Ceramic Society, 2020, 48(8): 1285-1294 (in Chinese).
[61] 王志航, 白二雷, 周俊鹏, 等. 玄武岩纤维增强地质聚合物混凝土的动态力学性能[J]. 振动与冲击, 2024, 43(19): 134-144.
WANG Z H, BAI E L, ZHOU J P, et al. Effects of basalt fibers and age on dynamic mechanical properties of geopolymer concrete[J]. Journal of Vibration and Shock, 2024, 43(19): 134-144 (in Chinese).
[62] WANG Z H, BAI E L, HUANG H, et al. Dynamic mechanical properties of carbon fiber reinforced geopolymer concrete at different ages[J]. Ceramics International, 2023, 49(1): 834-846.
[63] 于俊楠. 负温环境下路面快速修补用碱激发矿渣ECC性能研究[D]. 哈尔滨: 哈尔滨工业大学, 2020.
YU J N. Study on ECC performance of alkali-excited slag for quick pavement repair under negative temperature environment[D]. Harbin: Harbin Institute of Technology, 2020 (in Chinese).
[64] WANG Z H, BAI E L, REN B, et al. Effects of temperature and basalt fiber on the mechanical properties of geopolymer concrete under impact loads of different high strain rates[J]. Journal of Building Engineering, 2023, 72: 106605.
[65] 黄啸, 毛海勇, 袁晓峰, 等. -20 ℃条件下碱矿渣水泥性能研究[J]. 硅酸盐通报, 2014, 33(8): 2052-2055+2062.
HUANG X, MAO H Y, YUAN X F, et al. Research performance of AASC under the condition of -20 ℃[J]. Bulletin of the Chinese Ceramic Society, 2014, 33(8): 2052-2055+2062 (in Chinese).
[66] 邓鹏, 黄啸, 曹巨辉. 养护方式对负温条件下碱矿渣水泥砂浆强度的影响[J]. 材料导报, 2014, 28(增刊 2): 360-362+366.
DENG P, HUANG X, CAO J H. Impacts of maintenance methods on the strength of alkali-activated slag cement under negative temperature[J]. Materials Reports, 2014, 28(supplement 2): 360-362+366 (in Chinese).
[67] 吕炎, 白二雷, 王志航, 等. 低温制备硅灰-偏高岭土-矿渣基地聚物砂浆试验及微观研究[J]. 材料导报, 2023, 37(增刊 2): 218-226.
LYU Y, BAI E L, WANG Z H, et al. Experimental and microscopic study on preparation of silica fume-metakaolin-slag matrix polymer mortar at low temperature[J]. Materials Reports, 2023, 37(supplement 2): 218-226 (in Chinese).
[68] ZHANG H E, AI J H, REN Q, et al. Understanding the strength evolution of alkali-activated slag pastes cured at subzero temperature[J]. Cement and Concrete Composites, 2023, 138: 104993.
[69] 赵美杰. 碱激发矿渣胶凝材料的低温力学性能[D]. 哈尔滨: 哈尔滨工业大学, 2017.
ZHAO M J. Low temperature mechanical properties of alkali-excited slag gelling materials[D]. Harbin: Harbin Institute of Technology, 2017 (in Chinese).
[70] 李文博. 高性能套筒灌浆料的制备及低温环境的应用研究[D]. 郑州: 郑州大学, 2020.
LI W B. Preparation of high-performance sleeve grouting material and its application in low temperature environment[D]. Zhengzhou: Zhengzhou University, 2020 (in Chinese).
[71] 郝怡昕. CaO/硫铝酸盐水泥改性硅酸盐水泥的负温性能及机理研究[D]. 西安: 西安建筑科技大学, 2024.
HAO Y X. Study on negative temperature properties and mechanism of Portland cement modified by CaO/sulphoaluminate cement[D]. Xi’an: Xi’an University of Architecture and Technology, 2024 (in Chinese).
[72] 孙玉龙, 霍曼琳, 陈晓松. 负温铁路用预应力孔道压浆料的试验研究[J]. 新型建筑材料, 2020, 47(9): 123-126.
SUN Y L, HUO M L, CHEN X S. Experimental study on a prestressed passage grouting material for negative temperature railway[J]. New Building Materials, 2020, 47(9): 123-126 (in Chinese).
[73] 谢松, 朱清华, 钱冠龙, 等. 不同水泥基的低负温套筒灌浆料性能研究[J]. 新型建筑材料, 2020, 47(1): 47-49+66.
XIE S, ZHU Q H, QIAN G L, et al. Study on performance of low and negative temperature cementitious grout with different cement bases[J]. New Building Materials, 2020, 47(1): 47-49+66 (in Chinese).
[74] 谢松, 朱清华, 钱冠龙, 等. 利用硅酸盐水泥配制低温套筒灌浆料试验研究[J]. 新型建筑材料, 2019, 46(2): 15-18.
XIE S, ZHU Q H, QIAN G L, et al. Experimental study on making low temperature sleeve grouting material by using Portland cement[J]. New Building Materials, 2019, 46(2): 15-18 (in Chinese).
[75] 刘浩亚, 鲍洪志, 赵卫. -18 ℃下冻土区负温水泥浆水化微观过程研究[J]. 钻井液与完井液, 2019, 36(1): 77-81.
LIU H Y, BAO H Z, ZHAO W. Study on microscopic hydration process of a cold temperature cement slurry used in frozen areas at -18 ℃[J]. Drilling Fluid & Completion Fluid, 2019, 36(1): 77-81 (in Chinese).
[76] 刘浩亚, 赵卫, 李燕, 等. 负温早强水泥浆体系的室内实验[J]. 石油钻采工艺, 2019, 41(3): 294-300.
LIU H Y, ZHAO W, LI Y, et al. Laboratory experiments on the negative-temperature, early-strength slurry system[J]. Oil Drilling & Production Technology, 2019, 41(3): 294-300 (in Chinese).
[77] 刘浩亚, 鲍洪志, 刘亚青, 等. 改性高铝水泥浆的负温硬化性能及其增强机制[J]. 石油钻探技术, 2021, 49(2): 54-60.
LIU H Y, BAO H Z, LIU Y Q, et al. Hardening properties and enhancement mechanisms of modified alumina cement at minus temperature[J]. Petroleum Drilling Techniques, 2021, 49(2): 54-60 (in Chinese).
[78] 马正先, 周传贵, 杭鑫坤, 等. 矿物掺合料对负温套筒灌浆料性能的影响[J]. 混凝土与水泥制品, 2017(8): 80-83.
MA Z X, ZHOU C G, HANG X K, et al. Effects of mineral admixtures on properties of negative temperature sleeve grounting materials[J]. China Concrete and Cement Products, 2017(8): 80-83 (in Chinese).
[79] 马正先, 宋沛霖, 杭鑫坤, 等. 外加剂对负温套筒灌浆料性能的影响[J]. 混凝土, 2019(5): 142-146+150.
MA Z X, SONG P L, HANG X K, et al. Properties effect of admixture on negative temperature sleeve grouting material[J]. Concrete, 2019(5): 142-146+150 (in Chinese).
[80] 马正先, 周传贵, 杭鑫坤, 等. 水泥对负温套筒灌浆料性能的影响[J]. 混凝土, 2018(11): 152-156.
MA Z X, ZHOU C G, HANG X K, et al. Effect of composite cement on the properties of low temperature sleeve grouting material[J]. Concrete, 2018(11): 152-156 (in Chinese).
[81] 李兵, 马正先, 杭鑫坤, 等. 新型负温套筒灌浆料性能试验研究[J]. 混凝土与水泥制品, 2017(10): 9-13.
LI B, MA Z X, HANG X K, et al. Experimental research on properties of new kind of negative temperature cementitious grout[J]. China Concrete and Cement Products, 2017(10): 9-13 (in Chinese).
[82] 杭鑫坤. 低温套筒灌浆料试验研究[D]. 济南: 山东建筑大学, 2017.
HANG X K. Experimental research on low temperature sleeve grouting material[D]. Jinan: Shandong Jianzhu University, 2017 (in Chinese).