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BULLETIN OF THE CHINESE CERAMIC SOCIETY ›› 2010, Vol. 29 ›› Issue (1): 107-111.

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Preparation of Mn-doped Barium Titanate Nano-powder by Microwave-hydrothermal Method

MA Mai-xia;ZHANG Guang-xia   

  • Online:2010-02-15 Published:2021-01-18

Abstract: The Mn-doped barium titanate nano-powders were synthesized by Microwave-hydrothermal Method, in which Ti(OC_4H_9)_4 、Ba(NO_3)_2 and C_4H_6MnO_4·4H_2O compounds were used as raw materials. The Mn-doped Barium Titanate nano-powders were characterized by means of X-ray diffraction (XRD) and scanning electron microscope (SEM). The primary effects of processing parameters on the growth and morphology of the Mn-doped Barium Titanate were studied. The experimental results showed that the Mn-doped Barium Titanate of pure phase and uniform size was obtained when the concentration of Mn, the reaction time and drying temperature were 1.0%, 30 min and 82 ℃, respectively. And the size of the Mn-doped Barium Titanate powders was about 100 nm.

Key words: Mn-doped barium titanate;nano-powders;microwave-hydrothermal method

CLC Number: