真空玻璃支撑柱印刷烧结成型工艺及性能研究

硅酸盐通报 ›› 2022, Vol. 41 ›› Issue (4): 1157-1162.

• “玻璃材料与玻璃技术”专题 • 上一篇下一篇

真空玻璃支撑柱印刷烧结成型工艺及性能研究

赵广亮, 奚小波, 张翼夫, 张琦, 汪博文, 张剑峰, 张瑞宏

扬州大学机械工程学院,扬州 225127

收稿日期:2021-12-30 修回日期:2022-01-27 出版日期:2022-04-15 发布日期:2022-04-27
通讯作者: 奚小波,博士,讲师。E-mail:xxbctg@126.com
作者简介:赵广亮(1997—),男,硕士研究生。主要从事真空玻璃技术研究。E-mail:1505825373@qq.com
基金资助:
国家自然科学基金(51902284,52072334,52002349);扬州大学大学生学术科技创新基金(X20210363)

Printing Sintering Molding Process and Performance of Vacuum Glass Support Pillar

ZHAO Guangliang, XI Xiaobo, ZHANG Yifu, ZHANG Qi, WANG Bowen, ZHANG Jianfeng, ZHANG Ruihong

School of Mechanical Engineering, Yangzhou University, Yangzhou 225127, China

Received:2021-12-30 Revised:2022-01-27 Online:2022-04-15 Published:2022-04-27

摘要/Abstract

摘要： 传统真空玻璃支撑柱采用人工或机器布放,存在生产效率低、漏布率高等缺点。本文采用低熔点玻璃浆料印刷烧结制备支撑柱,优化了支撑柱印刷浆料调和浓度及印刷板参数,分析了不同烧结温度对支撑柱成型尺寸和强度的影响。结果表明,优化后的浆料调和浓度为5 g/mL,优化后的印刷板孔径为1.0 mm,厚度为0.5 mm,支撑柱最佳烧结温度为380 ℃,成型后支撑柱直径为1.25 mm,高度为0.23 mm,硬度达549.92 HV,性能较好。该研究对真空玻璃制造工艺具有指导意义。

关键词: 真空玻璃, 支撑柱, 印刷, 烧结成型, 玻璃粉, 浆料, 硬度

Abstract: The traditional vacuum glass support pillar is manually or mechanically arranged, which has the disadvantages of low production efficiency and high leakage rate. In this paper, a support pillar was prepared by printing sintering of low melting point glass slurry, the blending concentration and printed plate parameters of the support pillar printing slurry were optimized, and the effects of different sintering temperatures on the molding size and strength of the support pillar were analyzed. The results show that the optimized slurry blending concentration is 5 g/mL, the optimized pore size and thickness of the printed plate are 1.0 mm and 0.5 mm, the optimal sintering temperature of the support pillar is 380 ℃. The diameter of support pillar after molding is 1.25 mm, the height is 0.23 mm, the hardness is 549.92 HV, and the performance is good. This study has guiding significance for the vacuum glass manufacturing process.

Key words: vacuum glass, support pillar, printing, sintering molding, glass powder, slurry, hardness

中图分类号:

TQ171.7

赵广亮, 奚小波, 张翼夫, 张琦, 汪博文, 张剑峰, 张瑞宏. 真空玻璃支撑柱印刷烧结成型工艺及性能研究[J]. 硅酸盐通报, 2022, 41(4): 1157-1162.

ZHAO Guangliang, XI Xiaobo, ZHANG Yifu, ZHANG Qi, WANG Bowen, ZHANG Jianfeng, ZHANG Ruihong. Printing Sintering Molding Process and Performance of Vacuum Glass Support Pillar[J]. BULLETIN OF THE CHINESE CERAMIC SOCIETY, 2022, 41(4): 1157-1162.

参考文献

[1] 唐健正.真空玻璃[M].武汉:武汉理工大学出版社,2018.
TANG J Z. Vacuum glass[M]. Wuhan: Wuhan University of Technology Press, 2018 (in Chinese).
[2] COLLINS R E, ROBINSON S J. Evacuated glazing[J]. Solar Energy, 1991, 47(1): 27-38.
[3] COLLINS R E, SIMKO T M. Current status of the science and technology of vacuum glazing[J]. Solar Energy, 1998, 62(3): 189-213.
[4] 张凡,王晋珍,徐磊,等.玻璃-陶瓷基支撑点对真空玻璃力学性能及热导的影响[J].硅酸盐通报,2020,39(9):2974-2979.
ZHANG F, WANG J Z, XU L, et al. Effect of glass-ceramic based support pillars on mechanical properties and thermal conductivity of vacuum glass[J]. Bulletin of the Chinese Ceramic Society, 2020, 39(9): 2974-2979 (in Chinese).
[5] 陈鹏.钒碲铋系低熔点玻璃制备与真空玻璃封装工艺研究[D].武汉:武汉理工大学,2020.
CHEN P. Preparation of the low melting glass in the V₂O₅-TeO₂-Bi₂O₃ system and packaging technology of vacuum glazing[D]. Wuhan: Wuhan University of Technology, 2020 (in Chinese).
[6] 缪宏,左敦稳,张瑞宏,等.MATLAB的真空平板玻璃支撑柱应力数值分析[J].重庆建筑大学学报,2008,30(6):56-60.
MIAO H, ZUO D W, ZHANG R H, et al. A MATLAB-based numerical simulation analysis of shore stress in vacuum plate glass[J]. Journal of Chongqing Jianzhu University, 2008, 30(6): 56-60 (in Chinese).
[7] KIM Y, JEON E S. Establishment of regression model for estimating shape parameters for vacuum-sealed glass panel using design of experiments[J]. Vacuum, 2015, 121: 113-119.
[8] 顾乡,高建和,张瑞宏,等.真空平板玻璃支撑应力理论分析与实验研究[J].玻璃与搪瓷,2006,34(6):15-19+14.
GU X, GAO J H, ZHANG R H, et al. Theoretical analysis and experimental study on the brace stress of the vacuum glazing[J]. Glass & Enamel, 2006, 34(6): 15-19+14 (in Chinese).
[9] 李敏.全自动玻璃丝网印刷机印刷系统结构设计与分析[D].天津:天津职业技术师范大学,2021.
LI M. Structure design and analysis of automatic glass screen printing system[D]. Tianjin: Tianjin University of Technology and Education, 2021 (in Chinese).
[10] ZHANG R H. Effect of surface finish of braced pillars on stress distribution of vacuum plate glass[J]. Key Engineering Materials, 2010, 431/432: 450-453.
[11] 缪宏,张瑞宏,左敦稳,等.支撑柱对真空平板玻璃静态特性的影响[J].建筑材料学报,2013,16(1):153-158.
MIAO H, ZHANG R H, ZUO D W, et al. Effect of shore on static characteristics of vacuum plate glass[J]. Journal of Building Materials, 2013, 16(1): 153-158 (in Chinese).
[12] CHOI B, YEO I, LEE J, et al. Pillar-supported vacuum insulation panel with multi-layered filler material[J]. International Journal of Heat and Mass Transfer, 2016, 102: 902-910.
[13] 许嘉文,奚小波,张翼夫,等.支撑柱对钢化真空玻璃支撑应力影响仿真研究[J].计算机仿真,2021,38(8):291-298.
XU J W, XI X B, ZHANG Y F, et al. Simulation study on effect of support columns on stress of tempered vacuum glass[J]. Computer Simulation, 2021, 38(8): 291-298 (in Chinese).
[14] 孙诗兵,李金威,吕锋,等.β-锂霞石对Bi₂O₃-B₂O₃-ZnO系封接焊料封接粘结拉伸强度影响的研究[J].硅酸盐通报,2019,38(9):2960-2966.
SUN S B, LI J W, LYU F, et al. Tensile bonding strength of Bi₂O₃-B₂O₃-ZnO system sealing solder from β-eucryptite[J]. Bulletin of the Chinese Ceramic Society, 2019, 38(9): 2960-2966 (in Chinese).
[15] 赵晓丽.十二水合硫酸铝铵制备结晶氯化铝的研究[D].太原:山西大学,2019.
ZHAO X L. Study on the preparation of crystalline aluminum chloride by using ammonium aluminum sulfate[D]. Taiyuan: Shanxi University, 2019 (in Chinese).
[16] 奚小波,缪宏,金亦富,等.Ni-Co-Mn合金的电镀工艺优化及与金刚石复合镀的摩擦磨损性能[J].中国有色金属学报,2015,25(9):2523-2530.
XI X B, MIAO H, JIN Y F, et al. Electroplating process optimization of Ni-Co-Mn alloy and tribological wear performance of composition plating with diamond[J]. The Chinese Journal of Nonferrous Metals, 2015, 25(9): 2523-2530 (in Chinese).

真空玻璃支撑柱印刷烧结成型工艺及性能研究

Printing Sintering Molding Process and Performance of Vacuum Glass Support Pillar

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